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Rolls-Royce UTC

Department of Materials Science and Metallurgy

Studying at Cambridge

 

Differential Scanning Calorimeter (DSC)

We have a Netzsch DSC 404 high temperature differential scanning calorimeter, which is used to measure heat flow as a function of time and temperature. This allows us principally to determine phase transition temperatures and investigate phase transformation in the materials as a function of temperature, as well as to determine caloric values such as heat of transformation. Brief details of equipment:

  • Room temperature up to 1500°C
  • Inert argon / air / vacuum environment
  • Heating rate up to 50 K / min
  • Cooling rate up to 200 K / min

DSC, TGA & DTA thermal Analysis

 

Typically, samples are heated to melting and/or cooled from molten at a fixed rate of temperature change, and the heat flow measured as a function of temperature is used to determine phase transition temperatures. Example of test data generated:

DSC heating curves for the as-cast condition and after various solution heat treatment steps for single-crystal nickel-base superalloy CMSX-10K; from Pang, H.T., D’Souza, N., Dong, H., Stone, H.J., Rae, C.M.F., "Detailed Analysis of the Solution Heat Treatment of a Third-Generation Single-Crystal Nickel-Based Superalloy CMSX-10K®" (2016) Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science, 47 (2), pp. 889-906. DOI: 10.1007/s11661-015-3252-2

We also have a Setaram Setsys Evolution 18 equipment which could be used for Differential Thermal Analysis (DTA) measurements up to 1750°C

For further information and access, contact H.T. Pang.

RSS Feed Latest news

Dr. Lewis Owen appointed to a Junior Research Fellowship at Gonville & Caius College Cambridge

Jan 24, 2018

Dr. Lewis Owen has been appointed to a Junior Research Fellowship commencing in October 2018 at Gonville & Caius College Cambridge. We look forward to many more years of high quality research into the wonderful world of short range order.

Cambridge Academy for Science and Technology Visit

Jan 17, 2018

We had a fantastic time today hosting the uber-talented students from the Cambridge Academy for Science and Technology. We believe sharing some of our research and encouraging as many people as possible to consider STEM careers is a key responsibility for any scientist/engineer.

PhD studentships now available within the group

Jan 09, 2018

Navigate onto our vacancies page to find out more!

Strategic Partnership with Rolls-Royce shortlisted for a Times Higher Education Award 2017

Oct 03, 2017

The Rolls-Royce partnership with the universities of Cambridge, Swansea and Birmingham has been shortlisted for a Times Higher Education Award 2017. Find out more here: https://www.timeshighereducation.com/news/times-higher-education-awards-2017-shortlist-announced

New high temperature thermocouple

Nov 14, 2016

Dr. Michele Scervini has developed a new thermocouple for high-temperature applications